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1. (Article ID: 10360)
Lin LZ, Lin LJ, Cordell GA, Luo S, Jiang H
Spectral assignment of 2"-O-β-D-glucopyranosylsaikosaponin b2 by two-dimensional NMR techniques
Magnetic Resonance in Chemistry 30 (1992)
1097-1103
A new derivative of saikosaponin was isolated from the roots of Bupleurum longicaule and identified as 2″-O-β″-d-glucopyranosylsaikosaponin b2. Its 1H and 13C NMR data and the connectivities of the sugar moiety were assigned by use of a combination of two-dimensional NMR techniques (DQF-COSY, HOHAHA, ROESY, HETCOR and HMBC).
structure elucidation, separation, HOHAHA, ROESY, NMR assignment, triterpene saponin, 2"-O-β-d-glucopyranosylsaikosaponin b2, Bupleurum longicaule, 2D NMR (DQF-COSY, HETCOR, HMBC)
Journal NLM ID: 9882600Publisher: Wiley Heyden
Methods: NMR
The publication contains the following compound(s):
- Compound ID: 25203
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b-D-Glcp-(1-2)-b-D-Glcp-(1-3)-b-D-Fucp-(1-3)-Subst
Subst = saikogenin D = SMILES C[C@@]1({23}CO){3}[C@@H](O)CC[C@]2(C)[C@@]3([H])C=CC4=C5CC(C)(C)CC[C@@]({28}CO)5{16}[C@H](O)C[C@](C)4[C@@](C)3CC[C@@]12[H] |
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Structure type: oligomer
Trivial name: 2"-O-β"-D-glucopyranosylsaikosaponin-b2 saikosaponin, 2"-O-β-D-glucopyranosylsaikosaponin-b2
Compound class: saponin glycoside, glycoside, steroid glycoside
Reference(s) to other database(s): CCSD:
29774, CBank-STR:9531
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