Found 1 publication. Displayed publication 1
Expand all publications       Show all as text (SweetDB notation)
1. (Article ID: 12047)
 
Bonnländer B, Winterhalter P
9-Hydroxypiperitone β-D-glucopyranoside and other polar constituents from dill (Anethum graveolens L.) herb
Journal of Agricultural and Food Chemistry 48(10) (2000) 4821-4825
 

A methanolic extract from dill (Anethum graveolens) herb was subjected to XAD-2 adsorption chromatography. The methanolic eluate was fractionated with the all liquid chromatographic technique of multilayer coil countercurrent chromatography (MLCCC). After acetylation of MLCCC subfractions and flash chromatography, final purification of dill herb constituents was achieved by preparative and/or analytical HPLC. Nine compounds were obtained in pure form, including the beta-D-glucopyranosides of 9-hydroxypiperitone, p-menth-2-ene-1,6-diol, and 8-hydroxygeraniol. Structure elucidation is based on electrospray ionization ion trap multiple mass spectrometry (ESI-MS/MS) as well as one- and two-dimensional nuclear magnetic resonance spectroscopy.

glycosides, multilayer coil countercurrent chromatography, dill herb, 9-hydroxypiperitone β-D-glucopyranoside, p-menth-2-ene-1, 6-diol β-D-glucopyranoside, 8-hydroxygeraniol β-D-glucopyranoside, dill ether

The publication contains the following compound(s):
 

Expand this publication

Resort publications by:

New query Export IDs Home Help

Execution: <1 sec