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Structure type: oligomer
Aglycon: glycerol or 1,3-dioxolane/dioxane
Contained glycoepitopes: IEDB_136105,IEDB_142488,IEDB_144998,IEDB_146664,IEDB_158539,IEDB_225177,IEDB_885823,IEDB_983931,SB_192

• Article ID: 449
  Molinaro A, Evidente A, Lo Cantore P, Iacobellis NS, Bedini E, Lanzetta R, Parrilli M "Structural determination of a novel O-chain polysaccharide of the lipopolysaccharide from the bacterium Xanthomonas campestris pv. pruni" - European Journal of Organic Chemistry (12) (2003) 2254-2259
  

  In this paper, we report the structure of the O-specific polysaccharide of the LPS fraction of the strain type NCPPB416 of X. campestris pv. pruni. It is built up of three different monosaccharides glucose, rhamnose and xylose in an intricate block-wise polymer. Herein, the primary structure is elucidated by means of chemical degradation and 2D NMR spectroscopy.

  carbohydrates, polysaccharides, NMR spectroscopy, natural products

  Publication DOI: 10.1002/ejoc.200300051
  Journal NLM ID: 9805750
  Publisher: Wiley-VCH
  Correspondence: molinaro@unina.it
  Institutions: Dipartimento di Chimica Organica e Biochimica, Universita` di Napoli, Complesso Universitario Monte Sant Angelo, Via Cintia 4, 80126 Napoli, Italy, Dipartimento di Scienze del Suolo, della Pianta e dell'Ambiente, Universita` di Napoli ''Federico II'', Via Universita` 100, 80055 Portici, Italy, Dipartimento di Biologia, Difesa e Biotecnologie Agro Forestali, Universita` degli Studi della Basilicata, C. da Macchia Romana, 85100 Potenza, Italy
  Methods: NMR-2D, methylation, NMR, Smith degradation
  
   
  
  Xanthomonas campestris pv. pruni NCPPB416
  CSDB ID 9014 (all data & tools)