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1. (Article ID: 1828)
L'vov VL, Malikov VE, Shashkov AS, Dranovskaya EA, Dmitriev BA
Brucella somatic antigens. The structure of the O-specific polysaccharide chain of Brucella melitensis lipopolysaccharide
Bioorganicheskaya Khimia = Bioorganic Chemistry [Russian] 11(7) (1985)
963-969
The phenol-phase soluble antigenic lipopolysaccharide was isolated from Brucella melitensis, strain 565, by the routine phenol/water procedure followed by chromatography on Sepharose 4B. After mild acid hydrolysis and chromatography on Sephadex G-50, the lipopolysaccharide yielded a linear O-specific polysaccharide built up from 1,2-linked 4,6-dideoxy-4-formamido-α-D-mannopyranosyl units. The structure of the polysaccharide was deduced mainly from the nuclear magnetic resonance and methylation analyses. The phenol-soluble lipopolysaccharide, isolated from commercial vaccine strain B. abortus 19-BA, on mild hydrolysis afforded material, 13C and 1H-NMR spectra of which were identical to those of the O-specific polysaccharide from B. melitensis 565.
NCBI PubMed ID: 2413867Journal NLM ID: 7804941Publisher: Moskva: Nauka
Institutions: N.D. Zelinsky Institute of Organic Chemistry, Academy of Sciences of the USSR, Moscow, Russia
Methods: 13C NMR, 1H NMR
The publication contains the following compound(s):
- Compound ID: 866
Structure type: homopolymer
Trivial name: perosamine homopolymer, perosamine
Compound class: O-polysaccharide, O-antigen
Reference(s) to other database(s): GTC:G55700WU, GlycomeDB:
3393, CCSD:
42651, CBank-STR:4424
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