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1. (Article ID: 1857)
 
Knirel YA, Zdorovenko GM, Shashkov AS, Mamyan SS, Gubanova NY, Yakovleva LM, Solyanik LP
Antigenic polysaccharides of bacteria. 30. Structure of the polysaccharide chain of the Pseudomonas syringae pv. syringae 281 (serogroup I) lipopolysaccharide
Bioorganicheskaya Khimia = Bioorganic Chemistry [Russian] 14(2) (1988) 180-186
 

Anomeric methyl 3-O-(D-mannopyranosyl- and L-rhamnopyranosyl)-β-D-talopyranosides were synthesised by the stereoselective 1,2-cis- and 1,2-trans manno- and rhamnosylation of methyl 2,4,6-tri-O-acetyl-β-D-talopyranoside, which has been prepared from methyl β-D-galactopyranoside by a synthetic scheme including conversion of the C2 configuration. From 13C-NMR spectra of the disaccharides obtained the spectral alpha- and beta-effects of O3-glycosylation of talopyranose were determined.

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