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1. (Article ID: 197)
 
Vinogradov EV, Bock K, Petersen BO, Holst O, Brade H
The structure of the carbohydrate backbone of the lipopolysaccharide from Acinetobacter strain ATCC 17905
European Journal of Biochemistry 243(1-2) (1997) 122-127
 

The structure of the carbohydrate backbone of the lipopolysaccharide from Acinetobacter strain ATCC 17905 was studied. After deacylation of the lipopolysaccharide, a mixture of two compounds (ratio approximately 2:1) was isolated by high-performance anion-exchange chromatography, the structures of which were determined by NMR spectroscopy and electrospray-mass spectrometry as: [see formula in text] [Sug, 3-deoxy-D-manno-2-octulopyranosonic acid (Kdo) in oligosaccharide 1 (major portion) and D-glycero-D-talo-2-octulopyranosonic acid (Ko) in oligosaccharide 2 (minor portion)]. All monosaccharide residues also possess th D-cofiguration and are present in the pyranose form.

Lipopolysaccharide, NMR, Acinetobacter, core-lipid A region

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