The MeOH extract of the stem bark of Entada abyssinica and of the leaves and stem bark of Securidaca longipedunculata yielded a diterpene, a flavonol glycoside, and a phytosterol glycoside. Their structures were established on basis of NMR spectroscopic analysis; the complete 13C and 1H assignment of the compounds was achieved by means of 2D NMR studies.
diterpene, flavonol glycoside, Leguminosae, Polygalaceae, Securidaca longipedunculata, Entada abyssinica
Publication DOI: 10.1007/s007060050321Journal NLM ID: 0254164Publisher: Wien, New York: Springer-Verlag
Correspondence: haslinger@kfunigraaz.ac.at
Institutions: Institut für Pharmazeutische Chemie, Universität Graz, Graz, Austria, Schering AG Berlin, Berlin, Germany, Ethiopian Health and Nutrition Research Institute, Addis Ababa, Ethiopia, Institut für Pharmakognosie, Universität Graz, Graz, Austria
Methods: 13C NMR, 1H NMR, EI-MS, NMR-2D, FAB-MS, GC-MS, TLC, acid hydrolysis, LSI-MS, UV, extraction, CC, melting point determination, evaporation, PPC