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1. (Article ID: 3199)
Saksena R, Adamo R, Kovác P
Synthesis of the tetrasaccharide side chain of the major glycoprotein of the Bacillus anthracis exosporium
Bioorganic and Medicinal Chemistry Letters 16(3) (2006)
615-617
An alpha-glycoside of the tetrasaccharide sequence β-Ant-(1→3)-α-L-Rhap-(1→3)-α-L-Rhap-(1→2)-α-L-Rhap whose aglycon allows conjugation to suitable carriers was synthesized. The NMR characteristics of the compound are virtually identical with those of the α-anomer of the tetrasaccharide isolated from the major glycoprotein of the Bacillus anthracis exosporium. Thus, the correct structure of the natural product has been proven by chemical synthesis.
oligosaccharide, Anthrax, Anthrose, Exosporium glycoprotein, Thioglycoside
NCBI PubMed ID: 16275067Publication DOI: 10.1016/j.bmcl.2005.10.056Journal NLM ID: 9107377Publisher: Elsevier
Correspondence: kpn
helix.nih.gov
Institutions: National Institute of Diabetes and Digestive and Kidney Disease/LMC, National Institutes of Health, Bethesda, MD 20892-0815, USA
Methods: NMR, chemical methods
The publication contains the following compound(s):
- Compound ID: 7007
|
3HOiVl-(1-4)-b-D-Quip4N2Me-(1-3)-a-L-Rhap-(1-3)-a-L-Rhap-(1-2)-a-L-Rhap-(1--/->6) methyl 6-hydroxyhexanoate/
3HOiVl = 3-hydroxy-3-methylbutanoyl |
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Structure type: oligomer
Aglycon: ->6) methyl 6-hydroxyhexanoate
Trivial name: tetrasaccharide side chain of glycoprotein
Reference(s) to other database(s): GlycomeDB:
37212
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