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1. (Article ID: 3829)
Cai X, Zong G, Xu Y, Zhang J, Liang X, Wang D
Efficient synthesis of a 6-deoxytalose tetrasaccharide related to the antigenic O-polysaccharide produced by Aggregatibacter actinomycetemcomitans serotype c
Carbohydrate Research 345(9) (2010)
1230-1234
Concise synthesis of a 6-deoxy-α-L-talose tetrasaccharide, 6-deoxy-α-L-Talp-(1→3)-6-deoxy-α-L-Talp-(1→2)-6-deoxy-α-L-Talp-(1→3)-6-deoxy-α-L-Talp, the dimer of the disaccharide repeating unit of the OPS from Aggregatibacter actinomycetemcomitans serotype c, has been accomplished through suitable protecting group manipulations and stereoselective glycosylation starting from commercially available L-rhamnose. The target oligosaccharide in the form of its p-methoxyphenyl glycoside is suitable for further glycoconjugate formation via selective cleavage of this group.
tetrasaccharide, rhamnose, selective acylation, 6-deoxya-L-talose
NCBI PubMed ID: 20457448Journal NLM ID: 0043535Publisher: Elsevier
Correspondence: J. Zhang
cau.edu.cn>
Institutions: Key Lab of Pesticide Chemistry and Application Technology, Department of Applied Chemistry, China Agricultural University, Beijing, China
Methods: NMR, chemical synthesis, selective acylation
The publication contains the following compound(s):
- Compound ID: 8863
Structure type: polymer chemical repeating unit
Trivial name: c-specific polysaccharide antigen
Compound class: O-polysaccharide
Reference(s) to other database(s): GTC:G63295ZU
- Compound ID: 8864
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a-L-6dTalp-(1-3)-a-L-6dTalp-(1-2)-a-L-6dTalp-(1-3)-a-L-6dTalp-(1--/p-methoxyphenyl/ |
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Structure type: oligomer
Aglycon: p-methoxyphenyl
Reference(s) to other database(s): GTC:G96383IU
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