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1. (Article ID: 4590)
Pal KB, Mukhopadhyay B
Concise synthesis of the trisaccharide repeating unit of the O-polysaccharide from Aeromonas hydrophila A19 (O:14)
Carbohydrate Research 379 (2013)
26-29
Chemical synthesis of the trisaccharide repeating unit of the O-polysaccharide from Aeromonas hydrophila A19 (O:14) is reported in the form of its p-methoxyphenyl glycosides. Suitably protected monosaccharide synthons were prepared either by literature procedure or by strategies developed in house. Stereoselective glycosylations were accomplished by the activation of thioglycosides using N-iodosuccinimide in conjunction with H2SO4-silica in good to excellent yields.
glycosylation, H2SO4-silica, Bacterial oligosaccharides
NCBI PubMed ID: 23845517Publication DOI: 10.1016/j.carres.2013.06.009Journal NLM ID: 0043535Publisher: Elsevier
Correspondence: B. Mukhopadhyay
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Institutions: Department of Chemical Sciences, Indian Institute of Science Education and Research-Kolkata, Mohanpur, Nadia 741252, India
Methods: 13C NMR, 1H NMR, TLC, chemical synthesis, chemical methods, glycosylation
The publication contains the following compound(s):
- Compound ID: 9772
Structure type: polymer chemical repeating unit
Compound class: O-polysaccharide, O-antigen
Reference(s) to other database(s): GTC:G54049LH
- Compound ID: 11376
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a-L-Rhap-(1-4)-+
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a-D-Glcp-(1-2)-b-D-Glcp-(1--/p-methoxyphenyl/ |
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Structure type: oligomer
Aglycon: p-methoxyphenyl
Compound class: O-polysaccharide
Reference(s) to other database(s): GTC:G15543UF
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