Found 2 publications.
Displayed publications from 1 to 2
Expand all publications
Collapse all publications
Show all as text (SweetDB notation)
Show all graphically (SNFG notation)
1. (Article ID: 5031)
Pakiet K, Turska-Szewczuk A, Karaś MA, Pekala A, Pietras H
Structure of the O-specific polysaccharide from the lipopolysaccharide of Aeromonas hydrophila strain K691 containing 4-acetamido-4,6-dideoxy-D-glucose
Carbohydrate Research 439 (2017)
23-29
The O-specific polysaccharide (OPS) was isolated from the lipopolysaccharide of Aeromonas hydrophila strain K691 and studied by chemical methods and 1H and 13C NMR spectroscopy, including 2D 1H,1H COSY, TOCSY, NOESY, 1H-detected heteronuclear 1H,13C HSQC, and HMBC experiments. It was found that the O-specific polysaccharide was built up of pentasaccharide repeating units composed of β-GlcpNAc, 2-O-acetylated α-Rhap, and β-Quip4NAc residues. The following structure of the OPS was established: →3)-α-l-Rha2OAc-(1→3)-β-d-GlcNAc-(1→3)-α-l-Rha2OAc-(1→3)-β- d-GlcNAc-(1→2)-β-d-Qui4NAc-(1→.
LPS, O-antigen, O-specific polysaccharide, O-acetylation, 6-dideoxy-d-glucose, 4-amino-4, Aeromonas hydrophila, Fish pathogen
NCBI PubMed ID: 28088128Publication DOI: 10.1016/j.carres.2016.12.006Journal NLM ID: 0043535Publisher: Elsevier
Correspondence: aturska
hektor.umcs.lublin.pl
Institutions: Department of Genetics and Microbiology, M. Curie-Sklodowska University, Akademicka 19, 20-033 Lublin, Poland, Department of Fish Diseases, National Veterinary Research Institute, Partyzantów 57, 24-100 Pulawy, Poland
Methods: 13C NMR, 1H NMR, methylation, GLC-MS, NMR-2D, SDS-PAGE, sugar analysis, acid hydrolysis, GPC, reduction with NaBD4, N-acetylation
The publication contains the following compound(s):
Expand this publication
Collapse this publication
2. (Article ID: 5393)
Adak A, Mukhopadhyay B
Chemical synthesis of the 4-amino-4,6-dideoxy-D-glucose containing pentasaccharide repeating unit of the O-specific polysaccharide from Aeromonas hydrophila strain K691 in the form of its 2-aminoethyl glycoside
Carbohydrate Research 476(1) (2019)
1-7
Chemical synthesis of the pentasaccharide repeating unit of the O-specific polysaccharide from Aeromonas hydrophilastrain K691 is reported. Synthesis of the pentasaccharide is accomplished by using a common disaccharide in sequence and finally attaching the rare sugar unit. The target structure was made in the form of its 2-aminoethyl glycoside which is essential for further glycconjugate formation. Stereoselective glycosylations were achieved by the activation of thioglycosides in the presence of H2SO4-silica in conjunction with N-iodosuccinimide.
O-specific polysaccharide, 6-dideoxy-d-glucose, 4-amino-4, total synthesis, Fish pathogen, H(2)SO(4)-Silica
NCBI PubMed ID: 30861377Publication DOI: 10.1016/j.carres.2019.02.009Journal NLM ID: 0043535Publisher: Elsevier
Correspondence: B. Mukhopadhyay
iiserkol.ac.in>
Institutions: Sweet Lab, Department of Chemical Sciences, Indian Institute of Science Education and Research (IISER) Kolkata, Mohanpur, Nadia, 741246, India
Methods: 13C NMR, 1H NMR, TLC, chemical synthesis, optical rotation measurement, flash chromatography
The publication contains the following compound(s):
Expand this publication
Collapse this publication
Total list of publication IDs on all result pages of the current query:
Total list of corresponding CSDB IDs (permanent record IDs):
Execution: <1 sec