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1. (Article ID: 7995)
Rezanka T, Guschina IA
Glycoside esters from lichens of central Asia
Phytochemistry 58(3) (2001)
509-516
Ten compounds isolated from the extract of the central Asian lichens comprised new glycosides and glycoside esters having 18R-hydroxy-dihydroalloprotolichesterinic, 18S-hydroxy-dihydroprotolichesterinic and 18S-hydroxy-neodihydroprotolichesterinic acids, as the aglycones and a saccharide moiety linked at C-18 and also at C-21 made by glucose, xylose or rhamnose. The structures were elucidated using extensive spectroscopic analysis (1D and 2D NMR, MS, IR, UV and ORD) and by biochemical methods.
NMR, MS, glycoside esters, lichens of central Asia, IR, ORD, UV
NCBI PubMed ID: 11557085Publication DOI: 10.1016/S0031-9422(01)00261-8Journal NLM ID: 0151434Publisher: Elsevier
Correspondence: rezanka
biomed.cas.cz
Institutions: Institute of Ecology of the Volga River Basin of the Russian Academy of Sciences, Togliatti, Russia, Institute of Microbiology, Prague, Czech Republic
Methods: 13C NMR, 1H NMR, gel filtration, NMR-2D, IR, FAB-MS, GC-MS, TLC, acid hydrolysis, GC, HPLC, UV, extraction, optical rotation measurement, enzymatic assay, HR-FAB-MS, LR-FAB-MS
The publication contains the following compound(s):
- Compound ID: 20076
|
b-D-Glcp-(1-21)-Subst
Subst = 18S-hydroxyneodihydroprotolichesterinic acid = SMILES C{18}[C@H](O)CCCCCCCCCCCCC[C@@H]1OC(=O)[C@H](C)[C@H]1{21}C(=O)O |
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Structure type: monomer
; 533.6797 [M+H]+, 531 [M-H]-
C27H48O10
Compound class: glycoside
- Compound ID: 20077
|
b-D-Glcp-(1-18)-+
|
a-L-Rhap-(1-21)-Subst
Subst = 18R-hydroxydihydroalloprotolichesterinic acid = SMILES C{18}[C@@H](O)CCCCCCCCCCCCC[C@@H]1OC(=O)[C@H](C)[C@@H]1{21}C(=O)O |
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Structure type: oligomer
; 679.8234 [M+H]+, 677 [M-H]-
C33H58O14
Compound class: glycoside
- Compound ID: 20080
|
b-D-Glcp-(1-18)-+
|
b-D-Glcp-(1-21)-Subst
Subst = 18S-hydroxyneodihydroprotolichesterinic acid = SMILES C{18}[C@H](O)CCCCCCCCCCCCC[C@@H]1OC(=O)[C@H](C)[C@H]1{21}C(=O)O |
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Structure type: oligomer
; 695.8224 [M+H]+, 693 [M-H]-
C33H58O15
Compound class: glycoside
- Compound ID: 20074
|
a-L-Rhap-(1-21)-Subst
Subst = 18R-hydroxydihydroalloprotolichesterinic acid = SMILES C{18}[C@@H](O)CCCCCCCCCCCCC[C@@H]1OC(=O)[C@H](C)[C@@H]1{21}C(=O)O |
Show graphically |
Structure type: monomer
; 517.6801 [M+H]+, 515 [M-H]-
C27H48O9
Compound class: glycoside
- Compound ID: 20079
|
a-L-Rhap-(1-18)-+
|
b-D-Glcp-(1-21)-Subst
Subst = 18S-hydroxyneodihydroprotolichesterinic acid = SMILES C{18}[C@H](O)CCCCCCCCCCCCC[C@@H]1OC(=O)[C@H](C)[C@H]1{21}C(=O)O |
Show graphically |
Structure type: oligomer
; 679.8233 [M+H]+, 677 [M-H]-
C33H58O14
Compound class: glycoside
- Compound ID: 20075
|
b-D-Glcp-(1-21)-Subst
Subst = 18S-hydroxydihydroprotolichesterinic acid = SMILES C{18}[C@H](O)CCCCCCCCCCCCC[C@@H]1OC(=O)[C@@H](C)[C@H]1{21}C(=O)O |
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Structure type: monomer
; 533.6806 [M+H]+, 531 [M-H]-
C27H48O10
Compound class: glycoside
- Compound ID: 20078
|
b-D-Xylp-(1-18)-+
|
b-D-Glcp-(1-21)-Subst
Subst = 18S-hydroxydihydroprotolichesterinic acid = SMILES C{18}[C@H](O)CCCCCCCCCCCCC[C@@H]1OC(=O)[C@@H](C)[C@H]1{21}C(=O)O |
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Structure type: oligomer
; 665.7961 [M+H]+, 663 [M-H]-
C32H56O14
Compound class: glycoside
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2. (Article ID: 10858)
Rice KG, Wu P, Brand L, Lee YC
Experimental determination of oligosaccharide three-dimensional structure
Current Opinion in Structural Biology 3 (1993)
669-674
Journal NLM ID: 9107784Publisher: Elsevier
The publication contains the following compound(s):
- Compound ID: 26400
|
a-D-Manp-(1-3)-+ a-L-Fucp-(1-6)-+
| |
b-D-Xylp-(1-2)-b-D-Manp-(1-4)-b-D-GlcpNAc-(1-4)-D-GlcNAc
|
a-D-Manp-(1-6)-+ |
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Structure type: oligomer
Compound class: N-glycan
Reference(s) to other database(s): GTC:G36266PV, CCSD:
46364, CBank-STR:16026
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